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By using laser multiphoton ionization and a time-of-flight mass filter, we have detectednascent UF 5  from the 266 nm laser photodissociation of UF 6 , following a single laser firing.The method can be used to monitor these species under conditions wherein isotopically selective excitation is responsible for the dissociation of UF 6 .

“Single Shot” Laser Multiphoton Ionization Detection of UF5 Following the 266 nm Photodissociation of UF6

“Single Shot” Laser Multiphoton Ionization Detection of UF₅ Following the 266 nm Photodissociation of UF₆