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2,2-dimethylpentanedioic acid ( 2dmepdaH 2  ) and 3,3-dimethylpentanedioic acid ( 3dmepdaH 2  ) reacted with copper(II) acetate to give  [Cu(2dmepda)(H 2 O) 3 ] 2   ( 1 ) and  [Cu(3dmepda)(H 2 O) 3 ] 2   ( 2 ). Reaction of ( 1 ) and ( 2 ) with 1,10-phenanthroline and 2,2′-bipyridine yielded  [Cu(2dmepda)(phen)(H 2 O)] 2 0.5phen  ( 3 ),  [Cu(2dmepda)(bipy)(H 2 O)] 2   ( 4 ),  [Cu(2dmepda)(bipy)(EtOH)] 2 · 2EtOH  ( 4A ),  [Cu(3dmepda)(phen)(H 2 O)] 2   ( 5 ), and  [Cu(3dmepda)(bipy)(H 2 O)] 2 · ( 6 ) . The structures of ( 4A ) and ( 6 ) each consists of a  [Cu(bipy)(dicarboxylate)(solvent)] 2   dimer. The superoxide dismutase (SOD) mimetic activity of the novel copper complexes and their manganese analogues was investigated. The dimethyl sulphoxide(DMSO) soluble complexes ( 1 )–( 4 ) and ( 6 ) were assessed for their cancer chemotherapeutic potential towards hepatocellular carcinoma and kidney adenocarcinoma cell lines. The 1,10-phenanthroline containing complex  [Cu(2dmepda)(phen)(H 2 O)] 2 0.5phen  ( 3 ) was the most potent with activity that compares well to that of  cis platin.

bioinorganic chemistry and applications/bioinorganic chemistry and applications

Synthesis, Superoxide Dismutase Mimetic and Anticancer Activities of Metal Complexes of 2,2-Dimethylpentanedioic Acid(2dmepdaH<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" id="E1"><mml:mrow><mml:mn>2</mml:mn></mml:mrow></mml:math>) and 3,3-Dimethylpentanedioic acid(3dmepdaH<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" id="E2"><mml:mrow><mml:mn>2</mml:mn></mml:mrow></mml:math>): X-Ray Crystal Structures of [Cu(3dmepda)(bipy)]<mml:math xmlns:mml="http://www.w3.org/1998/Math/…

Synthesis, Superoxide Dismutase Mimetic and Anticancer Activities of Metal Complexes of 2,2-Dimethylpentanedioic Acid(2dmepdaH2) and 3,3-Dimethylpentanedioic acid(3dmepdaH2): X-Ray Crystal Structures of [Cu(3dmepda)(bipy)]