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Growth and Analysis of NSH and KMNSH Crystals by Slow Evaporation Technique
Author(s) -
V. Masilamani,
J. Shanthi,
V. Sheelarani
Publication year - 2014
Publication title -
isrn condensed matter physics
Language(s) - English
Resource type - Journals
eISSN - 2090-7400
pISSN - 2090-7397
DOI - 10.1155/2014/678567
Subject(s) - tetragonal crystal system , monoclinic crystal system , crystallography , crystal (programming language) , evaporation , nickel , crystal growth , potassium , materials science , magnesium , differential thermal analysis , crystal system , analytical chemistry (journal) , chemistry , crystal structure , diffraction , metallurgy , optics , physics , computer science , thermodynamics , programming language , chromatography
Nickel sulphate hexahydrate (NSH) and potassium magnesium nickel sulphate hexahydrate (KMNSH) single crystals were grown by slow evaporation method. The grown NSH crystal was found to crystallize in tetragonal system with space group P41 21 2 and KMNSH in monoclinic system with space group P121/c. The optical band gap energies of the grown crystals using UV-Vis spectral results for the doped and undoped NSH crystals were calculated. The presence of various functional groups in the crystal was identified by FTIR analysis. The thermal behaviour of the grown crystal has been studied by TGA/DTA analysis.

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