Synthesis of Triphenyltin (IV) and Dibutyltin (IV) Complexes of 1-Aryl-2,5-dithiohydrazodicarbonamides and Their Characterization | Zendy

Rashmi B. Rastogi | Zendy; Karuna Singh | Zendy; Vinay Jaiswal | Zendy

Open Access

Synthesis of Triphenyltin (IV) and Dibutyltin (IV) Complexes of 1-Aryl-2,5-dithiohydrazodicarbonamides and Their Characterization

Author(s) -

Rashmi B. Rastogi,

Karuna Singh,

Vinay Jaiswal

Publication year - 2014

Publication title -

journal of applied chemistry

Language(s) - English

Resource type - Journals

eISSN - 2314-6923

pISSN - 2356-7171

DOI - 10.1155/2014/529764

Subject(s) - chemistry , denticity , aryl , stoichiometry , infrared spectroscopy , mass spectrum , conductance , molar ratio , medicinal chemistry , infrared , spectral line , molar mass , polymer chemistry , stereochemistry , crystallography , catalysis , organic chemistry , ion , crystal structure , alkyl , physics , mathematics , polymer , combinatorics , astronomy , optics

Organotin complexes of the types Ph3SnL and Bu2SnL [where Ph = phenyl and Bu = butyl; HL = 1-phenyl-2,5-dithiohydrazodicarbonamide (HPhthc), 1-benzyl-2,5-dithiohydrazodicarbonamide (Hbzthc), 1-(4-ethoxyphenyl)-2,5-dithiohydrazodicarbonamide (HEtOPhthc)] have been prepared. Molar conductance studies demonstrate the nonionic behavior of the complexes. The 1H and 13C nuclear magnetic resonance and FAB mass spectra of the complexes are consistent with the proposed stoichiometry. Infrared spectra suggest an anionic bidentate coordinating behavior of the ligands

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