The Preparation and Structure of [(2,4-Dimethyl-8-ethyl-5,8-diazadec-4-ene-2-amine)chlorocopper(II)] Perchlorate | Zendy

Neil F. Curtis | Zendy; Jan L. Wikaira | Zendy

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The Preparation and Structure of [(2,4-Dimethyl-8-ethyl-5,8-diazadec-4-ene-2-amine)chlorocopper(II)] Perchlorate

Author(s) -

Neil F. Curtis,

Jan L. Wikaira

Publication year - 2013

Publication title -

journal of crystallography

Language(s) - English

Resource type - Journals

eISSN - 2356-7317

pISSN - 2314-5994

DOI - 10.1155/2013/753625

Subject(s) - perchlorate , chemistry , monoclinic crystal system , amine gas treating , medicinal chemistry , imine , chloride , diamine , copper , ion , inorganic chemistry , crystal structure , nuclear chemistry , polymer chemistry , organic chemistry , catalysis

Copper(II) chloride and perchlorate, N,N-diethylethane-1,2-diamine, react in (m)ethanol with acetone and ammonia to form [(2,4-dimethyl-8-ethyl-5,8-diazadec-4-ene-2-amine)chlorocopper(II)] perchlorate, C12H27Cl2CuN3O4, , monoclinic, C2/c, (Hall-C2/c); a, 26.418(1), b, 9.7385(4); c, 14.0993(5) Å; β, 91.134(3)°. This has copper(II) in tetrahedrally distorted square-planar coordination by one primary, one tertiary, and one imine nitrogen atom and the chloride ion

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