Efficient Synthesis and Characterization of Some Novel Nitro-Schiff Bases and Their Complexes of Nickel(II) and Copper(II) | Zendy

Hossein Naeimi | Zendy; Mohsen Moradian | Zendy

Open Access

Efficient Synthesis and Characterization of Some Novel Nitro-Schiff Bases and Their Complexes of Nickel(II) and Copper(II)

Author(s) -

Hossein Naeimi,

Mohsen Moradian

Publication year - 2012

Publication title -

journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.436

H-Index - 50

eISSN - 2090-9063

pISSN - 2090-9071

DOI - 10.1155/2013/701826

Subject(s) - chemistry , schiff base , imine , copper , nickel , transition metal , metal , nitro , proton nmr , nitrogen atom , polymer chemistry , characterization (materials science) , inorganic chemistry , crystallography , stereochemistry , group (periodic table) , organic chemistry , catalysis , nanotechnology , alkyl , materials science

Synthesis and characterization of some new Schiff base ligands derived from various diamines and nitrosalicylaldehyde and their complexes of Ni(II) and Cu(II) are reported. Several spectral techniques such as UV-Vis, FT-IR, and NMR spectra were used to identify the chemical structures of the reported ligands and their complexes. The ligands are found to be bound to the metal atom through the oxygen atoms of the hydroxyl groups and nitrogen atoms of imine groups, which is also supported by spectroscopic techniques. The results obtained by FT-IR and NMR showed that the Schiff base complexes of transition metal (II) have square-planar geometry

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