Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride | Zendy

Aydın Tavman | Zendy; Cemil İbiş | Zendy

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Spectral Characterization and Crystal Structure of 1,2-Bis-(1H-benzimidazol-2-yl)-ethane Dihydrochloride

Author(s) -

Aydın Tavman,

Cemil İbiş

Publication year - 2012

Publication title -

journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.436

H-Index - 50

eISSN - 2090-9063

pISSN - 2090-9071

DOI - 10.1155/2013/634986

Subject(s) - chemistry , crystal structure , characterization (materials science) , crystal (programming language) , medicinal chemistry , crystallography , stereochemistry , nanotechnology , materials science , computer science , programming language

The crystal structure of 1,2-bis-(1H-benzimidazol-2-yl)-ethane dihydrochloride (1) was determined by X-ray diffraction at room temperature. The structure of 1 was also characterized by mass, elemental analysis, FT-IR, and NMR spectroscopy techniques. The title compound crystallizes in triclinic system and space group P-1, a=7.1350, b=9.6299(1), c=15.3340(7) Å, α=80.67(2),β=79.66(2),γ=68.395(11)∘, V=958.33(10) Å3, Z=2. Owing to the anti conformations of –CH2– groups, the entire molecule is relatively flat. H1-NMR spectra of 1 show AA′XX′ system characteristics

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