English (United Kingdom)

https://curated-unify.zendy.io/wp-json/zendy-region/v1/featured_content/oa?rat=en

https://curated-unify.zendy.io/wp-json/zendy-region/v1/highlighted_journal/

Global: Zendy Plus annual

Presents the access of premium content as premium feature

Premium Content

Presents the keyphrase highlighting as premium feature

Keyphrase Highlighting

Presents the summarisation as premium feature

Summarisation

Insights

Presents the pdf analysis as premium feature

PDF Analysis

Presents the zaia usage as premium feature

ZAIA

Global: Zendy Plus monthly

Global: Zendy Tools annual

Global: Zendy Tools monthly

Global: Zendy Free Plan

Synthesis and characterization of microstructured crystalline complexes of [HgI2(C14H12N2)] and [HgBr2(C14H12N2)] were carried out from the reaction between 2,9-dimethyl-1,10-phenanthroline, mercury acetate, KI, and KBr, respectively, in methanol by sonochemical method. The reaction conditions were optimized under ultrasonic irradiations and without it. Characterization of the complexes was performed by elemental analysis, XRD, SEM, FTIR, and thermal analysis (TG/DTA). The results showed that sonochemical method caused significant reduction of the reaction time. Then the products were put under supercritical condition in a Teflon-lined, stainless-steel Parr bomb container and heated at 150°C for 48 h. The results showed that the chemical formulas of the complexes were not changed; however, the particle sizes were reduced and porosity increased

Synthesis and Characterization of Mercury(II) Complexes Containing 2,9-Dimethyl-1,10-phenanthroline by Sonochemical Method