Development and Characterization of Semi-IPN Silver Nanocomposite Hydrogels for Antibacterial Applications
Author(s) -
Amal Babu,
M. N. Prabhakar,
A. Suresh Babu,
B. Mallikarjuna,
M. C. S. Subha,
K. Chowdoji Rao
Publication year - 2013
Publication title -
international journal of carbohydrate chemistry
Language(s) - English
Resource type - Journals
eISSN - 1687-935X
pISSN - 1687-9341
DOI - 10.1155/2013/243695
Subject(s) - self healing hydrogels , silver nitrate , silver nanoparticle , carboxymethyl cellulose , nanocomposite , chemistry , scanning electron microscope , transmission electron microscopy , chemical engineering , radical polymerization , sulfonic acid , polymerization , polymer , polymer chemistry , nanoparticle , nuclear chemistry , nanotechnology , materials science , sodium , organic chemistry , composite material , engineering
Sodium carboxymethyl cellulose/poly(acrylamide-co-2-acrylamido-2-methylpropane sulfonic acid) semi-interpenetrating polymer network (semi-IPN) hydrogels were prepared by using free radical polymerization technique. Silver nanoparticles were formed by reduction of silver nitrate in semi-IPN hydrogels with sodium borohydrate at room temperature. UV-visible spectroscopy, thermogravimetrical analysis, X-ray diffractometry, scanning electron microscopy, and transmission electron microscopy techniques were used to characterize the formation of silver nanoparticles in hydrogels. SEM images indicated clearly the formation of group of silver nanoparticles with size range of 10–20 nm. The sizes of silver nanoparticles were also supported by transmission electron microscopy results. The semi-IPN silver nanocomposite hydrogels reported here might be a potentially smart material in the range of applications of antibacterial activity
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