Preparation and Characterization of P‐TSA Doped Tetraaniline Nanorods via Micellar‐Assisted Method | Zendy

K. Basavaiah | Zendy; A. V. Prasada Rao | Zendy

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Preparation and Characterization of P‐TSA Doped Tetraaniline Nanorods via Micellar‐Assisted Method

Author(s) -

K. Basavaiah,

A. V. Prasada Rao

Publication year - 2011

Publication title -

journal of chemistry

Language(s) - English

Resource type - Journals

eISSN - 2090-9063

pISSN - 2090-9071

DOI - 10.1155/2012/679462

Subject(s) - nanorod , chemistry , thermogravimetry , fourier transform infrared spectroscopy , scanning electron microscope , raman spectroscopy , dopant , nuclear chemistry , toluene , spectroscopy , doping , infrared spectroscopy , analytical chemistry (journal) , chemical engineering , nanotechnology , inorganic chemistry , organic chemistry , materials science , optics , physics , optoelectronics , quantum mechanics , engineering , composite material

In this work, we report preparation and characterization of P-toluene sulphonic acid (P-TSA) doped tetraaniline nanorods by micellar assisted method using ammonium per sulphate (APS) as an oxidant. Here, PTSA acts as dopant as well as template for tetraaniline nanostructures. The synthesized tetraaniline nanorods have been well characterized by Fourier transform infrared spectroscopy (FTIR), FT Raman spectroscopy, UV-Visible spectroscopy (UV-Visible), Scanning electron microscopy (SEM) and thermogravimetry. The morphologies of tetraaniline were found to be dependent on molar ratios of N-phenyl-1, 4-phenylenediamine (NPPD) to PTSA. The spectroscopic data indicated that PTSA doped tetraaniline nanorods. Thermogravimetry studies revealed that the PTSA doping improved the thermal stability of tetraaniline nanorods

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