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1Water and Steam Chemistry Division, Bhabha Atomic Research Centre Facilities, Kalpakkam 603102, India 2 Surface and Nanoscience Division, Indira Gandhi Centre for Atomic Research, Kalpakkam 603102, India 3 Institute of Semiconductor Physics, Russian Academy of Sciences, 630090 Novosibirsk, Russia 4Center for Condensed Matter Sciences, National Taiwan University, Taipei 106, Taiwan 5 Jawaharlal Nehru Centre for Advanced Scientific Research, International Centre for Materials Science and Chemistry, Bangalore 560064, India

Spectroscopic and Structural Insight into the Size-Dependent Behavior of the Nanophase