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The complex [ReOCl 3 pq] ( 1 ) (where pq = 2-(2′pyridyl)quinoxaline) has been synthesized and fully characterized by UV-Vis, FTIR, 1 and 2D NMR, and cyclic voltammetry (CV). The DNA-binding properties of the complex  1  as well as of the compounds [ReOCl 3 bpy] ( 2 ), [ReOCl 3 phen] ( 3 ), and pq ( 4 ) were investigated by UV-spectrophotometric (melting curves), CV (cyclic voltammetry), and viscosity measurements. Experimental data suggest that complex  1  intercalates into the DNA base pairs. Upon irradiation, complex  1  was found to promote the cleavage of plasmid pBR 322 DNA from supercoiled form I to nicked form II. The mechanism of the DNA cleavage by complex  1  was also investigated.

bioinorganic chemistry and applications/bioinorganic chemistry and applications

Synthesis, Characterization, DNA Binding, and Photocleavage Activity of Oxorhenium (V) Complexes with<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"><mml:mi>α</mml:mi></mml:math>-Diimine and Quinoxaline Ligands

Synthesis, Characterization, DNA Binding, and Photocleavage Activity of Oxorhenium (V) Complexes withα-Diimine and Quinoxaline Ligands