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One‐Step Route to Synthesize Multiwalled Carbon Nanotubes Filled with MgO Nanorods
Author(s) -
Jing Liu,
Chunli Guo,
Xiaojian Ma,
Changhui Sun,
Fengxia Li,
Yitai Qian
Publication year - 2010
Publication title -
journal of nanomaterials
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.463
H-Index - 66
eISSN - 1687-4129
pISSN - 1687-4110
DOI - 10.1155/2010/671863
Subject(s) - materials science , nanorod , crystallinity , raman spectroscopy , transmission electron microscopy , carbon nanotube , graphite , chemical engineering , morphology (biology) , carbon fibers , nanotechnology , composite material , composite number , optics , physics , engineering , biology , genetics
Multiwalled carbon nanotubes filled with MgO nanorods were synthesized through the reaction of ethanol and Mg powder in the presence of TiO2 at 400C°. X-ray powder diffraction indicated that the sample was composed of graphite and cubic MgO. Transmission electron microscopy studies showed that multi-walled CNTs with the outer diameters of 70–130 nm were filled with discontinuous MgO nanorods whose diameter was in the range of 25–40 nm. The ratios of the band intensities (ID/IG=0.67) in Raman spectrum implied that carbon nanotubes had good crystallinity. The influence of correlative reaction factors on the morphology of the sample and the possible formation mechanism were discussed

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