An Efficient Preparation, Spectroscopic Properties, and Crystal Structure of 1,1-Bis(4-[2-(dimethylamino)ethoxy]phenyl)-2-(3-guaiazulenyl)ethylene | Zendy

Shinichi Takekuma | Zendy; S. Hori | Zendy; Toshie Minematsu | Zendy; H. Takekuma | Zendy

Open Access

An Efficient Preparation, Spectroscopic Properties, and Crystal Structure of 1,1-Bis(4-[2-(dimethylamino)ethoxy]phenyl)-2-(3-guaiazulenyl)ethylene

Author(s) -

Shinichi Takekuma,

S. Hori,

Toshie Minematsu,

H. Takekuma

Publication year - 2009

Publication title -

research letters in organic chemistry

Language(s) - English

Resource type - Journals

eISSN - 1687-6938

pISSN - 1687-6865

DOI - 10.1155/2009/684359

Subject(s) - alkoxy group , yield (engineering) , crystal structure , molecule , crystal (programming language) , materials science , chemistry , crystallography , alkyl , computer science , organic chemistry , programming language , metallurgy

Reaction of 2-(3-guaiazulenyl)-1,1-bis(4-hydroxyphenyl)ethylene with 2-chloroethyldimethylammonium chloride in acetone in the presence of K2CO3 at reflux temperature for 24 hours gives a new title compound in 89% yield. Spectroscopic properties and crystal structure of the target molecule are reported

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