Study on Designing Sulfur Containing Bifunctional Building Block with Improved Refractive Index | Zendy

Gouri Shankar Jha | Zendy; Pranshu Chhabra | Zendy; Gunjan Suri | Zendy; M. Tyagi | Zendy; Pinklesh Arora | Zendy; Geetha Seshadri | Zendy; Rakesh Kumar Khandal | Zendy

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Study on Designing Sulfur Containing Bifunctional Building Block with Improved Refractive Index

Author(s) -

Gouri Shankar Jha,

Pranshu Chhabra,

Gunjan Suri,

M. Tyagi,

Pinklesh Arora,

Geetha Seshadri,

Rakesh Kumar Khandal

Publication year - 2008

Publication title -

journal of chemistry

Language(s) - English

Resource type - Journals

eISSN - 2090-9063

pISSN - 2090-9071

DOI - 10.1155/2009/634346

Subject(s) - bifunctional , chemistry , diol , exothermic reaction , fourier transform infrared spectroscopy , sulfur , reagent , chlorine , organic chemistry , chemical engineering , catalysis , engineering

Sulfur and chlorine containing bifunctional diols with C-S bond has been prepared starting from chloroepoxy alkane and thioalcohol. The studies of FTIR, TLC, HPLC and NMR have been used to understand the reaction mechanism, as well as for optimization of the reaction parameters. The reaction is highly exothermic and the effect of temperature, rate of addition of reagents and reaction time are important factors affecting the formation of diol. Viscosity studies, HPLC, FTIR, NMR and acid number studies have shown that, these parameters could be used as process control parameters for the synthesis of diol. Refractive index of the synthesized diol is found to be higher than that of the reactants used

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