Isolation, Synthesis and Characterization of Rosiglitazone Maleate Impurities | Zendy

S. Radha Krishna | Zendy; Mandava Venkata Naga Brahmeshwar Rao | Zendy; Tirmalaraju Satyanaryana Raju | Zendy; Vurimidi Himabindu | Zendy; Ghanta Mahesh Reddy | Zendy

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Isolation, Synthesis and Characterization of Rosiglitazone Maleate Impurities

Author(s) -

S. Radha Krishna,

Mandava Venkata Naga Brahmeshwar Rao,

Tirmalaraju Satyanaryana Raju,

Vurimidi Himabindu,

Ghanta Mahesh Reddy

Publication year - 2008

Publication title -

journal of chemistry

Language(s) - English

Resource type - Journals

eISSN - 2090-9063

pISSN - 2090-9071

DOI - 10.1155/2008/308724

Subject(s) - rosiglitazone , isolation (microbiology) , impurity , characterization (materials science) , chemistry , materials science , nanotechnology , biochemistry , biology , microbiology and biotechnology , organic chemistry , receptor

Three unknown impurities in rosiglitazone maleate 1 bulk drug at level below 0.1% (ranging from 0.05 to 0.1%) were detected by simple reverse phase high performance liquid chromatography. These impurities were preliminarily identified with LC-MS and characterized by the mass number of the impurities. Different experiments were conducted and finally synthesized and characterized the unknown impurities

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