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D-lyxono-γ-lactone has been prepared in two steps from galactose. The first step potassium lyxonate was obtained in 64% yield and the title compound has been isolated in next step with 75% yield. The structures of the products were characterized by IR, 1H, 13C, mass and microanalysis study

Synthesis and Characterization of D-Lyxono-γ-lactone