Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials | Zendy

Amanda L. Willis | Zendy; Zhuoying Chen | Zendy; Jiaqing He | Zendy; Yimei Zhu | Zendy; Nicholas J. Turro | Zendy; Stephen O’Brien | Zendy

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Metal Acetylacetonates as General Precursors for the Synthesis of Early Transition Metal Oxide Nanomaterials

Author(s) -

Amanda L. Willis,

Zhuoying Chen,

Jiaqing He,

Yimei Zhu,

Nicholas J. Turro,

Stephen O’Brien

Publication year - 2007

Publication title -

journal of nanomaterials

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.463

H-Index - 66

eISSN - 1687-4129

pISSN - 1687-4110

DOI - 10.1155/2007/14858

Subject(s) - nanocrystalline material , materials science , high resolution transmission electron microscopy , nanomaterials , transition metal , metal , oxide , transmission electron microscopy , chromium , nanoparticle , manganese , inorganic chemistry , chemical engineering , elemental analysis , nanotechnology , catalysis , metallurgy , organic chemistry , chemistry , engineering

A versatile, convenient, and nontoxic solvothermal method for the synthesis of nanocrystalline iron, chromium, and manganese oxides is described. This method employs the reactions of metal acetylacetonate precursors and oxygen-containing solvents in a reaction to prepare metal oxide nanoparticles. Characterization of these nanocrystalline materials was carried out employing transmission electron microscopy (TEM), high-resolution TEM (HRTEM), X-ray diffraction (XRD), and elemental analysis

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