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Titanium tetrachloride can be reduced by lanthanum filings to the corresponding low valent titanium complex, which can induce some aromatic aldehydes to the corresponding pinacols in 28%-97% yields within 10-50 min in ethyl acetate at r.t. under ultrasound irradiation

Pinacol Coupling of Aromatic Aldehydes using La-Ticl4in CH3COOEt under Ultrasound Irradiation

Pinacol Coupling of Aromatic Aldehydes using La-Ticl₄in CH₃COOEt under Ultrasound Irradiation