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Determination of Trace Metals with Newly Synthesized Coniine Dithiocarbamate by Atomic Absorption Spectroscopy
Author(s) -
Suvardhan Kanchi,
K. Suresh Kumar,
K. M. Reddy,
M Jyothi,
P. Chiranjeevi
Publication year - 2004
Publication title -
journal of chemistry
Language(s) - English
Resource type - Journals
eISSN - 2090-9063
pISSN - 2090-9071
DOI - 10.1155/2004/271531
Subject(s) - dithiocarbamate , atomic absorption spectroscopy , chemistry , elution , sorption , nuclear chemistry , polyurethane , chromatography , adsorption , organic chemistry , physics , quantum mechanics
A procedure is developed for the determination of Cd, Cu, Mo, Pb, Te and Ni in natural and spiked water by Atomic Absorption Spectroscopy (AAS) after preconcentration on a coniine dithiocarbamate supported by polyurethane. The sorbed elements are subsequently eluted with 5 mol L-1 HNO3 and the acid eluates are analysed by AAS. A 20 mL syringe served as a chromatographic preconcentration column. The sorption recoveries of elements were higher in the order of 99%. The method is also applied successfully for the determination of Cu, Cd, Mo, Pb, Te and Ni in natural and spiked water samples

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