Modeling of Binder Burnout and Sintering of Solid Oxide Electrolyte Tapes by Thermokinetic Analysis | Zendy

Axel C. Müller | Zendy

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Modeling of Binder Burnout and Sintering of Solid Oxide Electrolyte Tapes by Thermokinetic Analysis

Author(s) -

Axel C. Müller

Publication year - 2003

Publication title -

ecs proceedings volumes

Language(s) - English

Resource type - Journals

eISSN - 2576-1579

pISSN - 0161-6374

DOI - 10.1149/200307.0229pv

Subject(s) - sintering , materials science , electrolyte , thermogravimetry , yttria stabilized zirconia , burnout , oxide , composite material , chemical engineering , ceramic , metallurgy , cubic zirconia , chemistry , electrode , psychology , clinical psychology , engineering

Burnout of organic binder and sintering behavior of YSZ electrolyte green tapes were investigated by thermogravimetry and dilatometry, respectively. With the help of thermokinetic analysis burnout and sintering were described by a mathematical model based on formal kinetics. Thus the measured data were reduced to a set of a few parameters which can be easily used to simulate the kinetic behavior for an arbitrary temperature profile. Good accordance between prediction and respective measurement was accomplished. Using rate controlled binder burnout and rate controlled sintering, optimization of the temperature profile was achieved with respect to time and energy saving.

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