Method for Studying High Temperature Aqueous Electrochemical Systems: A Self Pressurized Autoclave | Zendy

Thomas R. Holm | Zendy; Per Kristian Dahlstrøm | Zendy; Svein Sunde | Zendy; David A. Harrington | Zendy; Frode Seland | Zendy

AI Assistant Blog Pricing

Home ZAIA Blog

Open Access

Method for Studying High Temperature Aqueous Electrochemical Systems: A Self Pressurized Autoclave

Author(s) -

Thomas R. Holm,

Per Kristian Dahlstrøm,

Svein Sunde,

David A. Harrington,

Frode Seland

Publication year - 2016

Publication title -

ecs transactions

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.235

H-Index - 52

eISSN - 1938-6737

pISSN - 1938-5862

DOI - 10.1149/07514.1055ecst

Subject(s) - autoclave , sulfuric acid , aqueous solution , electrolyte , electrochemistry , boiling , boiling point , materials science , electrode , current (fluid) , chemical engineering , chemistry , thermodynamics , metallurgy , engineering , organic chemistry , physics

A detailed description of a method using a self-pressurized autoclave to run aqueous electrochemical experiments at temperatures above the normal boiling point of water is given. Relevant challenges with studying electrochemical reactions at high current densities in such systems are identified, and potential methods for solving these challenges are provided. The method is demonstrated for a three-electrode setup in sulfuric acid electrolyte up to 140°C.

The content you want is available to Zendy users.

Already have an account? Click here to sign in.

Having issues? You can contact us here

Accelerating Research