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Nano-crystalline titanium diboride ( TiB  2 ) was prepared by self-propagating high-temperature synthesis through putting a hot filament on top of the compact mixture of TiO  2 , H  3  BO  3  and Mg with a stoichiometric ratio. Effects of the addition of various chloride salts e.g. NaClO  4  and NH  4  Cl as process control agents on phase evolution and chemical analysis and the morphology of the products were investigated by XRD and SEM techniques, respectively. Analysis of the X-ray diffraction patterns confirmed the formation of TiB  2  together with some intermediate phases such as Mg  3  B  2  O  6  and Mg  2  TiO  4  in as synthesized powder. MgO phase was detected as a major phase in the XRD patterns. Nano-crystalline TiB  2  became the major phase in some of the leached samples by HCl . The results also showed that the powder particle characteristics were influenced by the addition of the chloride salts.

EFFECTS OF PROCESS CONTROL AGENT ADDITION IN PROCESSING OF NANO-CRYSTALLINE TiB2 VIA SHS METHOD

EFFECTS OF PROCESS CONTROL AGENT ADDITION IN PROCESSING OF NANO-CRYSTALLINE TiB₂ VIA SHS METHOD