Redetermination of  N , N ′‐bis(4‐chlorophenyl)thiourea at 173 K | Zendy

Sarojini B. K. | Zendy; Narayana B. | Zendy; Swamy M. T. | Zendy; Yathirajan H. S. | Zendy; Bolte Michael | Zendy

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Redetermination of N , N ′‐bis(4‐chlorophenyl)thiourea at 173 K

Author(s) -

Sarojini B. K.,

Narayana B.,

Swamy M. T.,

Yathirajan H. S.,

Bolte Michael

Publication year - 2007

Publication title -

acta crystallographica section e

Language(s) - English

Resource type - Journals

ISSN - 1600-5368

DOI - 10.1107/s1600536807040871

Subject(s) - zigzag , thiourea , thio , crystallography , chemistry , hydrogen bond , urea , stereochemistry , bioinformatics , molecule , mathematics , geometry , organic chemistry , biology

The structure of the title compound, C 13 H 10 Cl 2 N 2 S, has already been determined at room temperature [Soriano‐García, Chávez, Cedillo, Pérez & Hernández (2001). Anal. Sci. 17 , 799–800]. However, the positions of the H atoms were not provided. Thus, we present here the complete structure determined from data at low temperature (173 K). The molecules are connected via bifurcated N—H...S hydrogen bonds to form zigzag chains running along the b axis. The title compound is isomorphous with 1,3‐bis(4‐bromophenyl)thiourea.

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