Powder study of 3‐azabicyclo[3.3.1]nonane‐2,4‐dione 1‐methylnaphthalene hemisolvate | Zendy

Hulme Ashley T | Zendy; Fernandes Philippe | Zendy; Johnston Andrea | Zendy; Florence Alastair | Zendy; Shankland Kenneth | Zendy

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Powder study of 3‐azabicyclo[3.3.1]nonane‐2,4‐dione 1‐methylnaphthalene hemisolvate

Author(s) -

Hulme Ashley T,

Fernandes Philippe,

Johnston Andrea,

Florence Alastair,

Shankland Kenneth

Publication year - 2006

Publication title -

acta crystallographica section e

Language(s) - English

Resource type - Journals

ISSN - 1600-5368

DOI - 10.1107/s1600536806030078

Subject(s) - nonane , rietveld refinement , naphthalene , powder diffraction , chemistry , high resolution , crystal structure , bicyclic molecule , crystallography , stereochemistry , organic chemistry , geology , remote sensing

The crystal structure of the title compound, C 8 H 11 N 1 O 2 ·0.5C 11 H 10 , was solved by simulated annealing from laboratory X‐ray powder diffraction data, collected at room temperature. Subsequent Rietveld refinement, using data collected to 1.51 Å resolution, yielded an R wp value of 0.057. The compound crystallizes with two molecules of 3‐azabicyclononane‐2,4‐dione and one molecule of 1‐methylnaphthalene in the asymmetric unit.

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