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An Intensified Esterification Process of Palm Oil Fatty Acid Distillate Catalyzed by Delipidated Rice Bran Lipase
Author(s) -
Fui Chin Chong,
Beng Ti Tey,
Zanariah Mohd Dom,
Nordin Ibrahim,
Russly Abd Rahman,
Tau Chuan Ling
Publication year - 2006
Publication title -
the scientific world journal
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.453
H-Index - 93
eISSN - 2356-6140
pISSN - 1537-744X
DOI - 10.1100/tsw.2006.213
Subject(s) - chemistry , lipase , palm oil , interesterified fat , glycerol , fatty acid , chromatography , distillation , rice bran oil , palm stearin , catalysis , candida antarctica , bran , organic chemistry , food science , enzyme , raw material
An intensified esterification process was operated by circulating 10 l of reaction mixtures, consisting of palm oil fatty acid distillate (PFAD) and glycerol in hexane, through a packed-bed reactor (PBR) filled with 10 kg of delipidated rice bran lipase (RBL). The influence of the process parameters, such as reaction temperature and type of water-removal agent, on the performance of this intensified esterification process were investigated. The highest degree of esterification (61%) was achieved at a reaction temperature of 65 masculineC, using silica gels as the water-removal agent. Thin-layer chromatography (TLC) analysis showed that the major composition of the esterified product was diacylglycerol.

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