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Progress in aberration-corrected scanning transmission electron microscopy
Author(s) -
Niklas Dellby,
O. L. Krivanek,
P.D. Nellist,
P. E. Batson,
Andrew R. Lupini
Publication year - 2001
Publication title -
microscopy
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.545
H-Index - 52
eISSN - 2050-5701
pISSN - 2050-5698
DOI - 10.1093/jmicro/50.3.177
Subject(s) - scanning transmission electron microscopy , optics , spherical aberration , contrast transfer function , microscope , resolution (logic) , point (geometry) , dark field microscopy , materials science , conventional transmission electron microscope , physics , scanning electron microscope , microscopy , computer science , mathematics , geometry , artificial intelligence , lens (geology)
A new corrector of spherical aberration (C(S)) for a dedicated scanning transmission electron microscope (STEM) is described and its results are presented. The corrector uses strong octupoles and increases C(C) by only 0.2 mm relative to the uncorrected microscope. Its overall stability is greatly improved compared to our previous design. It has achieved a point-to-point resolution of 1.23 A in high-angle annular dark field images at 100 kV. It has also increased the current available in a 1.3 A-sized probe by about a factor of ten compared to existing STEMs. Its operation is greatly assisted by newly developed autotuning software which measures all the aberration coefficients up to fifth order in less than one minute. We conclude by discussing the present limits of aberration-corrected STEM, and likely future developments.

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