High-throughput powder diffraction measurement system consisting of multiple MYTHEN detectors at beamline BL02B2 of SPring-8 | Zendy

Shogo Kawaguchi | Zendy; Michitaka Takemoto | Zendy; Kunihiko Osaka | Zendy; Eiji Nishibori | Zendy; Chikako Moriyoshi | Zendy; Yoshiki Kubota | Zendy; Yoshihiro Kuroiwa | Zendy; Kunihisa Sugimoto | Zendy

Open Access

High-throughput powder diffraction measurement system consisting of multiple MYTHEN detectors at beamline BL02B2 of SPring-8

Author(s) -

Shogo Kawaguchi,

Michitaka Takemoto,

Kunihiko Osaka,

Eiji Nishibori,

Chikako Moriyoshi,

Yoshiki Kubota,

Yoshihiro Kuroiwa,

Kunihisa Sugimoto

Publication year - 2017

Publication title -

review of scientific instruments

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.605

H-Index - 165

eISSN - 1089-7623

pISSN - 0034-6748

DOI - 10.1063/1.4999454

Subject(s) - beamline , nist , detector , materials science , powder diffraction , system of measurement , diffraction , optics , computer science , beam (structure) , physics , nuclear magnetic resonance , astronomy , natural language processing

In this study, we developed a user-friendly automatic powder diffraction measurement system for Debye–Scherrer geometry using a capillary sample at beamline BL02B2 of SPring-8. The measurement system consists of six one-dimensional solid-state (MYTHEN) detectors, a compact auto-sampler, wide-range temperature control systems, and a gas handling system. This system enables to do the automatic measurement of temperature dependence of the diffraction patterns for multiple samples. We introduced two measurement modes in the MYTHEN system and developed new attachments for the sample environment such as a gas handling system. The measurement modes and the attachments can offer in situ and/or time-resolved measurements in an extended temperature range between 25 K and 1473 K and various gas atmospheres and pressures. The results of the commissioning and performance measurements using reference materials (NIST CeO2 674b and Si 640c), V2O3 and Ti2O3, and a nanoporous coordination polymer are presented

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