Development of in-situ sample cells for scanning transmission x-ray microscopy | Zendy

Takuji Ohigashi | Zendy; Masanari Nagasaka | Zendy; Toshio Horigome | Zendy; Nobuhiro Kosugi | Zendy; Scott M. Rosendahl | Zendy; Adam P. Hitchcock | Zendy

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Development of in-situ sample cells for scanning transmission x-ray microscopy

Author(s) -

Takuji Ohigashi,

Masanari Nagasaka,

Toshio Horigome,

Nobuhiro Kosugi,

Scott M. Rosendahl,

Adam P. Hitchcock

Publication year - 2016

Publication title -

aip conference proceedings

Language(s) - English

Resource type - Conference proceedings

SCImago Journal Rank - 0.177

H-Index - 75

eISSN - 1551-7616

pISSN - 0094-243X

DOI - 10.1063/1.4952922

Subject(s) - in situ , materials science , microscopy , polarization (electrochemistry) , synchrotron , electrochemistry , analytical chemistry (journal) , optics , electrode , chemistry , physics , organic chemistry , chromatography

An azimuthal rotatable sample cell, an electrochemical cell and a controlled humidity cell for in-situ scanning transmission X-ray microscopy (STXM) were developed at UVSOR-III Synchrotron (Okazaki, Japan). By using these sample cells, the polarization dependence of sodium titanate nanoribbons, in-situ electrochemistry of 0.1M FeSO4 solution, and in-situ morphological change of a functional polymer with changing humidity were successfully measured.

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