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Magnetic hyperthermia heating of cobalt ferrite nanoparticles prepared by low temperature ferrous sulfate based method
Author(s) -
Tejabhiram Yadavalli,
Hardik Jain,
Gopalakrishnan Chandrasekharan,
Ramasamy Chennakesavulu
Publication year - 2016
Publication title -
aip advances
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.421
H-Index - 58
ISSN - 2158-3226
DOI - 10.1063/1.4942951
Subject(s) - spinel , materials science , ferrous , cobalt , nanoparticle , ferrite (magnet) , coprecipitation , nanostructure , chemical engineering , scanning electron microscope , ferromagnetism , atmospheric temperature range , analytical chemistry (journal) , nanotechnology , metallurgy , composite material , chemistry , physics , chromatography , quantum mechanics , meteorology , engineering
A facile low temperature co-precipitation method for the synthesis of crystalline cobalt ferrite nanostructures using ferrous sulfate salt as the precursor has been discussed. The prepared samples were compared with nanoparticles prepared by conventional co-precipitation and hydrothermal methods using ferric nitrate as the precursor. X-ray diffraction studies confirmed the formation of cubic spinel cobalt ferrites when dried at 110 °C as opposed to conventional methods which required higher temperatures/pressure for the formation of the same. Field emission scanning electron microscope studies of these powders revealed the formation of nearly spherical nanostructures in the size range of 20-30 nm which were comparable to those prepared by conventional methods. Magnetic measurements confirmed the ferromagnetic nature of the cobalt ferrites with low magnetic remanance. Further magnetic hyperthermia studies of nanostructures prepared by low temperature method showed a rise in temperature to 50 °C in 600 s

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