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The photocatalytic properties of different calcium tantalate nanocomposite photocatalysts with optimized phase composition were studied without the addition of any co-catalysts in the photoreforming of different alcohols including the biomass conversion by-product glycerol, as well as after modification with double-layered NiO<inf>x</inf> (Ni/NiO) co-catalyst in overall water splitting (OWS). Nanocomposite photocatalyst consisting of cubic α-CaTa<inf>2</inf>O<inf>6</inf>/orthorhombic β-CaTa<inf>2</inf>O<inf>6</inf> coexisting phases always possesses the highest photocatalytic performance. For overall water splitting, a loading of 0.5 wt. % NiO<inf>x</inf> exhibits the best activities with stable stoichiometric H<inf>2</inf> and O<inf>2</inf> evolution rates. &#169; 2015 Author(s)close0

New insight into calcium tantalate nanocomposite photocatalysts for overall water splitting and reforming of alcohols and biomass derivatives