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Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
Author(s) -
P.C. Lansåker,
Anders Hallén,
Gunnar A. Niklasson,
Claes G. Granqvist
Publication year - 2014
Publication title -
aip advances
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.421
H-Index - 58
ISSN - 2158-3226
DOI - 10.1063/1.4897340
Subject(s) - scanning electron microscope , rutherford backscattering spectrometry , materials science , characterization (materials science) , nanoparticle , spectroscopy , microscopy , analytical chemistry (journal) , sputter deposition , substrate (aquarium) , colloidal gold , energy dispersive x ray spectroscopy , nanotechnology , thin film , sputtering , optics , chemistry , physics , composite material , oceanography , chromatography , quantum mechanics , geology
Gold nanoparticle films are of interest in several branches of science and technology,and accurate sample characterization is needed but technically demanding. We preparedsuch films by DC magnetron sputtering and recorded their mass thicknessby Rutherford backscattering spectroscopy. The geometric thickness dg—from thesubstrate to the tops of the nanoparticles—was obtained by scanning electron microscopy(SEM) combined with image analysis as well as by atomic force microscopy(AFM). The various techniques yielded an internally consistent characterization ofthe films. In particular, very similar results for dg were obtained by SEM with imageanalysis and by AFM.EU GRINDOO

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