Synthesis and characterization of Ni(II) complex with 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-7,14-dienium bromide | Zendy

Latifah M. Yusoff | Zendy; Siti Fairus M. Yusoff | Zendy; Mohamad Wafiuddin Ismail | Zendy; Bohari M. Yamin | Zendy

Open Access

Synthesis and characterization of Ni(II) complex with 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-7,14-dienium bromide

Author(s) -

Latifah M. Yusoff,

Siti Fairus M. Yusoff,

Mohamad Wafiuddin Ismail,

Bohari M. Yamin

Publication year - 2014

Publication title -

aip conference proceedings

Language(s) - English

Resource type - Conference proceedings

eISSN - 1551-7616

pISSN - 0094-243X

DOI - 10.1063/1.4895222

Subject(s) - nickel , bromide , fourier transform infrared spectroscopy , chemistry , ligand (biochemistry) , ring (chemistry) , fourier transform , crystal structure , characterization (materials science) , infrared , elemental analysis , crystallography , nuclear chemistry , materials science , inorganic chemistry , optics , organic chemistry , physics , nanotechnology , biochemistry , receptor , quantum mechanics

Nickel(II) complex have been synthesized by treating a 14-membered ring tetraaza macrocyclic compound, 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-7,14-dienium, bromide (Me6N4H4)Br2 with nickel acetate in metanol. The complex was characterized using elemental analysis, Fourier Transform Infrared (FTIR), Ultraviolet-Visible (UV-Vis), and single crystal diffraction (X-ray). The nickel atom coordinates through four nitrogen atoms in the ligand. Square planar geometry has been proposed for this complex.

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