Tailored polyaniline/barium strontium titanate/expanded graphite multiphase composite for efficient radar absorption
Author(s) -
Pradeep Sambyal,
Avanish Pratap Singh,
Meenakshi Verma,
M. Farukh,
Bhanu Pratap Singh,
S. Dhawan
Publication year - 2014
Publication title -
rsc advances
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.746
H-Index - 148
ISSN - 2046-2069
DOI - 10.1039/c3ra46479b
Subject(s) - reflection loss , materials science , polyaniline , microwave , electromagnetic shielding , barium titanate , composite number , graphite , absorption (acoustics) , raman spectroscopy , dielectric , strontium titanate , dielectric loss , analytical chemistry (journal) , composite material , optics , optoelectronics , polymer , chemistry , polymerization , telecommunications , physics , computer science , chromatography
The present paper reports the synthesis of a high-performance microwave absorbing material using a simple, cost-effective and scalable method by encapsulating barium strontium titanate (BST) and expanded graphite (EG) in a polyaniline (PANI) matrix. One of the formulations (higher content of BST) shows shielding effectiveness due to absorption of more than 50 dB (>99.9999% attenuation) with minimum reflection loss (≤1 dB) in the Ku-band (12.4–18 GHz) frequency range. Another formulation (higher content of EG) shows a total shielding effectiveness of more than 81 dB with a reflection loss of 10 dB. In order to probe the relationship between the observed shielding response and the electromagnetic attributes, dielectric and permeability parameters have been calculated from the measured scattering parameters (S11, S22, S12, S21) using the Nicolson–Ross–Weir algorithm. The synthesised formulations were characterized thoroughly using XRD, FTIR, TGA, UV, Raman spectroscopy, SEM and HRTEM.
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