Poly(ethylene glycol) as reaction medium for mild Mizoroki–Heck reaction in a ball-mill | Zendy

Valérie Declerck | Zendy; Evelina Colacino | Zendy; Xavier Bantreil | Zendy; Jean Martínez | Zendy; Frédéric Lamaty | Zendy

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Poly(ethylene glycol) as reaction medium for mild Mizoroki–Heck reaction in a ball-mill

Author(s) -

Valérie Declerck,

Evelina Colacino,

Xavier Bantreil,

Jean Martínez,

Frédéric Lamaty

Publication year - 2012

Publication title -

chemical communications

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.837

H-Index - 333

eISSN - 1364-548X

pISSN - 1359-7345

DOI - 10.1039/c2cc36286d

Subject(s) - polyethylene glycol , ethylene glycol , ball mill , heck reaction , phosphine , palladium , chemistry , peg ratio , polymer chemistry , catalysis , nuclear chemistry , chemical engineering , materials science , organic chemistry , metallurgy , finance , economics , engineering

Phosphine-free palladium-catalyzed Mizoroki-Heck reaction was performed using ball-milling in polyethylene glycol under mild conditions. Good to excellent yields of coupling products were obtained. This activation technique also allowed the concomitant formation of round shaped Pd-PEG nanoparticles that were characterized by TEM analysis.

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