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The new binuclear chromium Pacman complex [Cr 2 (L)] of the Schiff base pyrrole macrocycle H 4 L has been synthesized and structurally characterized. Addition of isocyanide, C≡NR (R = xylyl, t Bu), or triphenylphosphine oxide donors to [Cr 2 (L)] gives contrasting chemistry with the formation of the new coordination compounds [Cr 2 (μ-CNR)(L)], in which the isocyanides bridge the two Cr(II) centers, and [Cr 2 (OPPh 3 ) 2 (L)], a Cr(II) phosphine oxide adduct with the ligands exogenous to the cleft.

Isocyanide and Phosphine Oxide Coordination in Binuclear Chromium Pacman Complexes