A Sm(II)-Mediated Cascade Approach to Dibenzoindolo[3,2-b]carbazoles: Synthesis and Evaluation | Zendy

Matthew T. Levick | Zendy; Iain Grace | Zendy; ShengYao Dai | Zendy; Nicholas Kasch | Zendy; C.A. Muryn | Zendy; Colin J. Lambert | Zendy; Michael L. Turner | Zendy; David J. Procter | Zendy

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A Sm(II)-Mediated Cascade Approach to Dibenzoindolo[3,2-b]carbazoles: Synthesis and Evaluation

Author(s) -

Matthew T. Levick,

Iain Grace,

ShengYao Dai,

Nicholas Kasch,

C.A. Muryn,

Colin J. Lambert,

Michael L. Turner,

David J. Procter

Publication year - 2014

Publication title -

organic letters

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.94

H-Index - 239

eISSN - 1523-7060

pISSN - 1523-7052

DOI - 10.1021/ol500841b

Subject(s) - chemistry , cascade , cyclic voltammetry , cleavage (geology) , combinatorial chemistry , spectroscopy , phase (matter) , stereochemistry , organic chemistry , electrochemistry , electrode , materials science , chromatography , physics , composite material , quantum mechanics , fracture (geology)

Previously unstudied dibenzoindolo[3,2-b]carbazoles have been prepared by two-directional, phase tag-assisted synthesis utilizing a connective-Pummerer cyclization and a SmI2-mediated tag cleavage-cyclization cascade. The use of a phase tag allows us to exploit unstable intermediates that would otherwise need to be avoided. The novel materials were characterized by X-ray, cyclic voltammetry, UV-vis spectroscopy, TGA, and DSC. Preliminary studies on the performance of OFET devices are also described.

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