Chemoenzymatic Halocyclization of 4-Pentenoic Acid at Preparative Scale | Zendy

Georg T. Höfler | Zendy; Andrada But | Zendy; Sabry H. H. Younes | Zendy; Ron Wever | Zendy; Caroline E. Paul | Zendy; Isabel W. C. E. Arends | Zendy; Frank Hollmann | Zendy

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Chemoenzymatic Halocyclization of 4-Pentenoic Acid at Preparative Scale

Author(s) -

Georg T. Höfler,

Andrada But,

Sabry H. H. Younes,

Ron Wever,

Caroline E. Paul,

Isabel W. C. E. Arends,

Frank Hollmann

Publication year - 2020

Publication title -

acs sustainable chemistry and engineering

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.878

H-Index - 109

ISSN - 2168-0485

DOI - 10.1021/acssuschemeng.9b07494

Subject(s) - scale (ratio) , chemistry , biochemical engineering , current (fluid) , identification (biology) , scale up , biological system , combinatorial chemistry , chromatography , organic chemistry , nanotechnology , materials science , biology , engineering , physics , thermodynamics , ecology , classical mechanics , quantum mechanics

The scale-up of chemoenzymatic bromolactonization to 100 g scale is presented, together with an identification of current limitations. The preparative-scale reaction also allowed for meaningful mass balances identifying current bottlenecks of the chemoenzymatic reaction.

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