Ionically Tagged Magnetic Nanoparticles with Urea Linkers: Application for Preparation of 2-Aryl-quinoline-4-carboxylic Acids via an Anomeric-Based Oxidation Mechanism | Zendy

Parvin Ghasemi | Zendy; Meysam Yarie | Zendy; Mohammad Ali Zolfigol | Zendy; Avat Taherpour | Zendy; Morteza Torabi | Zendy

Open Access

Ionically Tagged Magnetic Nanoparticles with Urea Linkers: Application for Preparation of 2-Aryl-quinoline-4-carboxylic Acids via an Anomeric-Based Oxidation Mechanism

Author(s) -

Parvin Ghasemi,

Meysam Yarie,

Mohammad Ali Zolfigol,

Avat Taherpour,

Morteza Torabi

Publication year - 2020

Publication title -

acs omega

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.779

H-Index - 40

ISSN - 2470-1343

DOI - 10.1021/acsomega.9b03277

Subject(s) - quinoline , thermogravimetric analysis , chemistry , aryl , carboxylic acid , sulfonic acid , magnetic nanoparticles , fourier transform infrared spectroscopy , nanoparticle , polymer chemistry , organic chemistry , materials science , chemical engineering , nanotechnology , alkyl , engineering

In this exploration, we reported the design and synthesis of a novel ionically tagged magnetic nanoparticles bearing urea linkers, namely, Fe 3 O 4 @SiO 2 @(CH 2 ) 3 -urea-thiazole sulfonic acid chloride. The structure of the mentioned compound was fully characterized by using several techniques including Fourier transform infrared spectroscopy, energy-dispersive X-ray analysis, elemental mapping analysis, thermogravimetric analysis/differential thermal analysis, scanning electron microscopy, transmission electron microscopy, and vibrating sample magnetometer. In the presence of the novel reusable catalyst, applied starting materials including aryl aldehydes, pyruvic acid, and 1-naphthylamine condensed to afford the desired 2-aryl-quinoline-4-carboxylic acid derivatives via an anomeric-based oxidation pathway under solvent-free conditions.

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