Reduced to Hierarchy: Carbon Filament-Supported Mixed Metal Oxide Nanoparticles | Zendy

G. V. Manohara | Zendy; Andrew Whiting | Zendy; H. Chris Greenwell | Zendy

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Reduced to Hierarchy: Carbon Filament-Supported Mixed Metal Oxide Nanoparticles

Author(s) -

G. V. Manohara,

Andrew Whiting,

H. Chris Greenwell

Publication year - 2019

Publication title -

acs omega

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.779

H-Index - 40

ISSN - 2470-1343

DOI - 10.1021/acsomega.9b02534

Subject(s) - oxide , materials science , carbon fibers , hydroxide , nanoparticle , raman spectroscopy , protein filament , chemical engineering , pyrolysis , metal , thermal treatment , inorganic chemistry , nanotechnology , chemistry , composite material , metallurgy , composite number , physics , engineering , optics

We describe a one-pot synthesis method for carbon filament-supported mixed metal oxide nanoparticles. The thermal intracrystalline reaction of adamantanecarboxylate ions confined inside interlayer galleries of layered double hydroxide materials under a reducing atmosphere (H) leads to carbon filaments forming in situ within the material. Raman spectroscopy and combined microscopy techniques show the formation of hybrid organic-inorganic carbon filaments with the mixed metal oxide particles interleaved.

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