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A group of novel 1,4-bis(3,5-dialkyl-4 H -1,2,4-triazol-4-yl)benzene and 5-aryltriaz-1-en-1-yl-1-phenyl-1 H -pyrazole-4-carbonitrile derivatives have been successfully synthesized and characterized by spectroscopic analyses. The triazenes were obtained in moderate yield by a coupling reaction between 5-aminopyrazol-4-carbonitrile and aryl diazonium chlorides, and their structures were confirmed by detecting the CN functional group in both IR and 13 C NMR spectra. Conversely, the novel 1,4-bis(3,5-dialkyl-4 H -1,2,4-triazol-4-yl)benzene derivatives were obtained using a previously unreported and facile pathway starting with p -phenylenediamine with selected triethyl orthoalkylates and then hydrazine monohydrate, followed by refluxing in triethyl orthoalkylates. The structure of the methyl derivative was confirmed by X-ray analysis. The synthesized compounds were tested and evaluated as antimicrobial agents.

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Facile Synthesis and Antimicrobial Activities of Novel 1,4-Bis(3,5-dialkyl-4<i>H</i>-1,2,4-triazol-4-yl)benzene and 5-Aryltriaz-1-en-1-yl-1-phenyl-1<i>H</i>-pyrazole-4-carbonitrile Derivatives

Facile Synthesis and Antimicrobial Activities of Novel 1,4-Bis(3,5-dialkyl-4H-1,2,4-triazol-4-yl)benzene and 5-Aryltriaz-1-en-1-yl-1-phenyl-1H-pyrazole-4-carbonitrile Derivatives