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Herein we report the iron-catalyzed β-C (sp 3 )-methylation of primary alcohols using methanol as a C1 building block. This borrowing hydrogen approach employs a well-defined bench-stable (cyclopentadienone)iron(0) carbonyl complex as precatalyst (5 mol %) and enables a diverse selection of substituted 2-arylethanols to undergo β-C (sp 3 )-methylation in good isolated yields (24 examples, 65% average yield).

Iron-Catalyzed Borrowing Hydrogen β-C(sp3)-Methylation of Alcohols

Iron-Catalyzed Borrowing Hydrogen β-C(sp³)-Methylation of Alcohols