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Particulate matter and NO  x  emissions from diesel exhaust remains one of the most pressing environmental problems. We explore the use of hierarchically ordered mixed Fe-Ce-Zr oxides for the simultaneous capture and oxidation of soot and reduction of NO  x  by ammonia in a single step. The optimized material can effectively trap the model soot particles in its open macroporous structure and oxidize the soot below 400 °C while completely removing NO in the 285-420 °C range. Surface characterization and DFT calculations emphasize the defective nature of Fe-doped ceria. The isolated Fe ions and associated oxygen vacancies catalyze facile NO reduction to N 2 . A mechanism for the reduction of NO with NH 3 on Fe-doped ceria is proposed involving adsorbed O 2 . Such adsorbed O 2 species will also contribute to the oxidation of soot.

Simultaneous NOx and Particulate Matter Removal from Diesel Exhaust by Hierarchical Fe-Doped Ce–Zr Oxide

Simultaneous NO_x and Particulate Matter Removal from Diesel Exhaust by Hierarchical Fe-Doped Ce–Zr Oxide