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One-pot processes for the synthesis of benzo[ b ]furans from 1-aryl- or 1-alkylketones using nonprecious transition metal catalysts have been developed. Regioselective iron(III)-catalyzed halogenation of the aryl ring, followed by iron- or copper-catalyzed O -arylation allowed the synthesis of various structural analogues, including the benzo[ b ]furan-derived natural products corsifuran C, moracin F, and caleprunin B.

Synthesis of Benzo[b]furans by Intramolecular C–O Bond Formation Using Iron and Copper Catalysis