Selective, Scalable Synthesis of C60-Fullerene/Indene Monoadducts Using a Microwave Flow Applicator | Zendy

Joshua P. Barham | Zendy; Satoko Tanaka | Zendy; Emiko Koyama | Zendy; Noriyuki Ohneda | Zendy; Tadashi Okamoto | Zendy; Hiromichi Odajima | Zendy; Junichi Sugiyama | Zendy; Yasuo Norikane | Zendy

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Selective, Scalable Synthesis of C₆₀-Fullerene/Indene Monoadducts Using a Microwave Flow Applicator

Author(s) -

Joshua P. Barham,

Satoko Tanaka,

Emiko Koyama,

Noriyuki Ohneda,

Tadashi Okamoto,

Hiromichi Odajima,

Junichi Sugiyama,

Yasuo Norikane

Publication year - 2018

Publication title -

the journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.2

H-Index - 228

eISSN - 1520-6904

pISSN - 0022-3263

DOI - 10.1021/acs.joc.7b03209

Subject(s) - indene , chemistry , fullerene , microwave , residence time (fluid dynamics) , selectivity , flow chemistry , solvent , continuous flow , scalability , acceptor , photochemistry , nanotechnology , organic chemistry , catalysis , materials science , telecommunications , biochemical engineering , computer science , physics , geotechnical engineering , database , engineering , condensed matter physics

The synergy of continuous processing and microwave heating technologies has unlocked scalable (g/h), safe and efficient reaction conditions for synthesis of fullerene/indene-based organic photovoltaic acceptor materials in a nonchlorinated solvent with levels of productivity unparalleled by previous syntheses. The microwave flow reactor sustains high temperature while employing short residence times, reaction conditions which uniquely allow the selective synthesis of fullerene/indene monoadducts. Design of experiments analysis revealed residence time as the most crucial factor for conversion and selectivity control.

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