Flow Synthesis of Diaryliodonium Triflates | Zendy

Gabriele Laudadio | Zendy; Hannes P. L. Gemoets | Zendy; Volker Hessel | Zendy; Timothy Noël | Zendy

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Flow Synthesis of Diaryliodonium Triflates

Author(s) -

Gabriele Laudadio,

Hannes P. L. Gemoets,

Volker Hessel,

Timothy Noël

Publication year - 2017

Publication title -

the journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.2

H-Index - 228

eISSN - 1520-6904

pISSN - 0022-3263

DOI - 10.1021/acs.joc.7b01346

Subject(s) - chemistry , flow chemistry , continuous flow , scalability , flow (mathematics) , combinatorial chemistry , residence time (fluid dynamics) , scale (ratio) , nanotechnology , organic chemistry , catalysis , biochemical engineering , computer science , mechanics , database , physics , materials science , geotechnical engineering , quantum mechanics , engineering

A safe and scalable synthesis of diaryliodonium triflates was achieved using a practical continuous-flow design. A wide array of electron-rich to electron-deficient arenes could readily be transformed to their respective diaryliodonium salts on a gram scale, with residence times varying from 2 to 60 s (44 examples).

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