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Fundamental Investigation of the Drying of Solid Suspensions
Author(s) -
Abdulkadir Osman,
Lucas Goehring,
Alessandro Patti,
E. Hugh Stitt,
Nima Shokri
Publication year - 2017
Publication title -
industrial and engineering chemistry research
Language(s) - English
Resource type - Journals
eISSN - 1520-5045
pISSN - 0888-5885
DOI - 10.1021/acs.iecr.7b02334
Subject(s) - scanning electron microscope , particle (ecology) , materials science , work (physics) , particle size , colloid , microstructure , volume (thermodynamics) , chemical engineering , nanotechnology , composite material , thermodynamics , physics , oceanography , engineering , geology
In this work, a comprehensive series of experiments is conducted to investigate the drying behavior of micro- and nanosized particle dispersions. To this end, an acoustic levitator was used to study the drying kinetics of single droplets. The temporal evolution of the actual droplets was recorded using a complementary metal oxide semiconductor (CMOS) camera, and the solid grains produced at the end of drying were investigated by scanning electron microscopy (SEM) imaging. At the end of drying, the grains show different morphologies as a function of the particle size, concentration, and initial droplet volume. We combine these experimental data to show the drying behavior is dependent on all the parameters and that the data all collapse when plotted against the Peclet number. This resulted in a novel characteristic diagram which allows one to predict the shape of the dried colloidal droplet based on Pe. Our results extend the fundamental understanding of the mechanisms controlling the drying of droplet sus...

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