Time-Resolved Powder X-ray Diffraction of the Solvothermal Crystallization of Cobalt Gallate Spinel Photocatalyst Reveals Transient Layered Double Hydroxides | Zendy

Daniel S. Cook | Zendy; Yue Wu | Zendy; Karla Lienau | Zendy; René Moré | Zendy; Reza J. Kashtiban | Zendy; Oxana V. Magdysyuk | Zendy; Greta R. Patzke | Zendy; Richard I. Walton | Zendy

Open Access

Time-Resolved Powder X-ray Diffraction of the Solvothermal Crystallization of Cobalt Gallate Spinel Photocatalyst Reveals Transient Layered Double Hydroxides

Author(s) -

Daniel S. Cook,

Yue Wu,

Karla Lienau,

René Moré,

Reza J. Kashtiban,

Oxana V. Magdysyuk,

Greta R. Patzke,

Richard I. Walton

Publication year - 2017

Publication title -

chemistry of materials

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 3.741

H-Index - 375

eISSN - 1520-5002

pISSN - 0897-4756

DOI - 10.1021/acs.chemmater.7b01761

Subject(s) - library science , citation , art history , history , computer science , materials science , physics , analytical chemistry (journal) , nanotechnology , chemistry , chromatography

High energy X-ray diffraction is used to follow in situ the crystallization of a cobalt gallate from metallic gallium under solvothermal conditions in an aminoalcohol, revealing the formation and decay of transient metastable layered double hydroxides. Photocatalytic studies show the spinel product has activity as a water oxidation catalyst for oxygen evolution

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