Synthesis, spectroscopic and crystal structure analysis of 2-(4-fluorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole and its morpholinomethyl derivative | Zendy

Afshan Banu | Zendy; D.E. Vasundhara | Zendy; Ravi S. Lamani | Zendy; Imtiyaz Ahmed M. Khazi | Zendy; Noor Shahina Begum | Zendy

Open Access

Synthesis, spectroscopic and crystal structure analysis of 2-(4-fluorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole and its morpholinomethyl derivative

Author(s) -

Afshan Banu,

D.E. Vasundhara,

Ravi S. Lamani,

Imtiyaz Ahmed M. Khazi,

Noor Shahina Begum

Publication year - 2011

Publication title -

journal of saudi chemical society

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.67

H-Index - 47

eISSN - 2212-4640

pISSN - 1319-6103

DOI - 10.1016/j.jscs.2011.03.010

Subject(s) - chemistry , stacking , intermolecular force , supramolecular chemistry , crystal structure , crystal (programming language) , crystallography , stereochemistry , elemental analysis , derivative (finance) , infrared spectroscopy , proton nmr , molecule , organic chemistry , computer science , financial economics , programming language , economics

The preparation of 2-(4-fluorobenzyl)-6-(4-methoxyphenyl)-5-morpholin-1-ylmethyl imidazo[2,1-b][1,3,4]thiadiazole via the intermediate 2-(4-fluorobenzyl)-6-(4-methoxyphenyl)Imidazo[2,1-b][1,3,4] thiadiazole is described. Elemental analysis, IR spectrum, 1H NMR and X-ray crystal structure analyses were carried out to determine the compositions and molecular structures of the two compounds. The crystal packing exhibits intermolecular C–H?O, C–H?N, C–H?F and π–π stacking interactions leading to the formation of the supramolecular network

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