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Influence of phase volume fraction on the grain refining of a Ti-6Al-4V alloy by high-pressure torsion
Author(s) -
Jie Fu,
Hua Ding,
Yi Huang,
Wenjing Zhang,
Terence G. Langdon
Publication year - 2014
Publication title -
journal of materials research and technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.832
H-Index - 44
eISSN - 2214-0697
pISSN - 2238-7854
DOI - 10.1016/j.jmrt.2014.10.006
Subject(s) - equiaxed crystals , materials science , lamellar structure , volume fraction , grain size , alloy , torsion (gastropod) , indentation hardness , phase (matter) , metallurgy , composite material , microstructure , chemistry , medicine , surgery , organic chemistry
A cold-rolled Ti-6Al-4V sheet was subjected to three different heat treatments prior to processing by high pressure torsion (HPT). Quantitative measurements revealed that the volume fractions were 70% equiaxed α phase and 30% lamellar (α+β) (Ti64-1), 47% equiaxed α phase and 53% lamellar (α+β) (Ti64-2) and 25% equiaxed α phase and 75% lamellar (α+β) (Ti64-3) and the grain sizes of the α phase were 7.0±2μm, 9.0±1.5μm and 9.5±1.5μm, respectively. The processing by HPT was performed at room temperature with a pressure of 6.0GPa and a rotation speed of 1rpm. Processing of the three heat treatment batches was conducted through a total number of revolutions, N, of 1/4, 1, 5, 10 and 20. The results show that the microhardness increases with increasing numbers of turns in HPT processing and for all three conditions stable microhardness values are reached after about 20 turns. The grain sizes after 20 turns of HPT were 115±30nm in Ti64-1, 85±25nm in Ti64-2 and 75±15nm in Ti64-3 so that the grain size decreases as the volume fraction of α phase decreases and the lamellar (α+β) increases

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